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<publisher>HAL CCSD</publisher>
<title lang=en>Analysis of semi-volatile organic compounds in indoor suspended particulate matter by thermal desorption coupled with gas chromatography/mass spectrometry.</title>
<creator>Mercier, Fabien</creator>
<creator>Glorennec, Philippe</creator>
<creator>Blanchard, Olivier</creator>
<creator>Le Bot, Barbara</creator>
<contributor>Laboratoire d'étude et de recherche en environnement et santé (LERES) ; École des Hautes Études en Santé Publique [EHESP] (EHESP)</contributor>
<contributor>Institut de recherche, santé, environnement et travail [Rennes] (Irset) ; Université d'Angers (UA) - Université des Antilles et de la Guyane (UAG) - Université de Rennes 1 (UR1) - École des Hautes Études en Santé Publique [EHESP] (EHESP) - Institut National de la Santé et de la Recherche Médicale (INSERM) - Structure Fédérative de Recherche en Biologie et Santé de Rennes ( Biosit : Biologie - Santé - Innovation Technologique )</contributor>
<contributor>French Ministry of Health (DGS)</contributor>
<description>International audience</description>
<source>ISSN: 0021-9673</source>
<source>Journal of Chromatography A</source>
<publisher>Elsevier</publisher>
<identifier>hal-00732133</identifier>
<identifier>https://hal.archives-ouvertes.fr/hal-00732133</identifier>
<source>https://hal.archives-ouvertes.fr/hal-00732133</source>
<source>Journal of Chromatography A, Elsevier, 2012, 1254, pp.107-14. 〈10.1016/j.chroma.2012.07.025〉</source>
<identifier>DOI : 10.1016/j.chroma.2012.07.025</identifier>
<relation>info:eu-repo/semantics/altIdentifier/doi/10.1016/j.chroma.2012.07.025</relation>
<identifier>PUBMED : 22840824</identifier>
<relation>info:eu-repo/semantics/altIdentifier/pmid/22840824</relation>
<language>en</language>
<subject lang=en>Thermal desorption</subject>
<subject lang=en>GC/MS</subject>
<subject lang=en>SVOCs</subject>
<subject lang=en>Suspended particulate matter</subject>
<subject lang=en>Indoor air</subject>
<subject>[SDV.SPEE] Life Sciences [q-bio]/Santé publique et épidémiologie</subject>
<type>info:eu-repo/semantics/article</type>
<type>Journal articles</type>
<description lang=en>People are exposed to multiple pollutants, especially indoors. In the perspective of a cumulative risk assessment, a multi-residue analytical method was developed to assess the contamination of indoor suspended particulate matter by 55 semi-volatile organic compounds (SVOCs) including musk fragrances, organochlorines (OCs), organophosphates (OPs), polycyclic aromatic hydrocarbons (PAHs), polybromodiphenylethers (PBDEs), polychlorobiphenyls (PCBs), phthalates and pyrethroids. It is based on thermal desorption (TD) coupled with gas chromatography/mass spectrometry (GC/MS). Once the thermal desorption conditions were optimized, the method was validated in terms of quantification limits and accuracy using a standard reference material (SRM 2585). Instrumental quantification limits were 10pg (some OCs, some pyrethroids, musk fragrances, OPs, PAHs, PBDEs and PCBs), 100pg (phthalates and other OCs) and 1000pg (other pyrethroids) corresponding respectively to method quantification limits of 1, 10, and 100pg/m(3) for a sampled air volume of 20m(3). Calibration quadratic curves for ranges of 10-1000, 100-10,000, and 1000-100,000pg, depending on the substance, exhibit determination coefficients above 0.999. Recoveries were between 61 and 96% for chlorinated pesticides, PAHs, PBDEs and PCBs present in the SRM 2585. A test of the method on indoor particulate matter samples (PM(10)) collected on quartz fiber filters in French dwellings demonstrated its ability to quantify SVOCs from a small amount of PM.</description>
<date>2012-09-07</date>
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